*.*.44.201
药智数据企业版
量身打造,体验升级
立即前往
VIP免费试用申请
登录 注册
当前位置: 首页 > 化合物提纯方法 > α-Cyclodextrin (H2O) 反馈纠错 帮助中心 打印
英文名 α-Cyclodextrin (H2O)
类型 碳水化合物
CAS号 10016-20-3
物理性质 M 972.9, m >280℃(dec), [α]546 +175℃ (c 10, H2O).
提纯方法 Recrystallise α-cyclodextrin from 60% aqueous EtOH, then twice from water, and dry it for 12hours in a vacuum at 80℃. It is also purified by precipitation from water with 1,1,2-trichloroethylene. The precipitate is collected, washed and resuspended in water. This is boiled to steam distil the trichloroethylene. The solution is then freeze-dried to recover the cyclodextrin. [Armstrong et al. J Am Chem Soc 108 1418 1986]. [Beilstein 19/12 V 789.]
相关文献 暂无权限
数据更新时间:2024-11-07
扩展信息

发布